MTSS Handbook

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Author: Gary Buchenic
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Price: $27.00

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New mesoporous materials

These materials, known as MTSs (Micelle Templated Silicas) can be prepared with a range of pore sizes (see Figure 4.4). As the pore size is essentially the diameter of the micelle template, it is easy to estimate the pore size obtained with a given template. For example, a MTS made with a dodecyl trialkylammonium (C12) template would have a pore diameter approximately twice the length of the dodecyl trialkylammonium species - roughly 2.2nm. As the chain length of the template molecules decreases, there comes a point where they do not form micelles. This happens around C8, meaning that the smallest pores achievable using this method are around 1.8 nm. Luckily, this is almost ideal in many ways, since the largest zeolites have pore sizes of c. 1.3 nm, almost seamlessly extending the range of pore sizes available to the chemist. At the other extreme, as the chain length increases, the ability of the quaternary salt to form micelles decreases, due to lack of solubility, and the largest...

Applications

The initial applications of MTSs were, perhaps not surprisingly, simply attempts to reproduce zeolite chemistry on larger molecules. This chemistry is based on the fact that the aluminium centres in zeolites cause a negative charge to exist on the framework of the solid this charge must be balanced by a cation. When the cation is a hydrogen ion (proton), the material is an acid, and indeed some zeolites are very strong acids indeed. However, the acidity of the corresponding MTSs is much lower, and initially this limited their applicability somewhat. Nevertheless, the MTSs are often found to be very effective as mild acid catalysts. Much work has therefore been aimed at the production of other materials using the same concept, but with either different templating systems, or with combinations of elements other than Si and Al in the framework. existing processes being far from 'green'. Thus researchers have been active in preparing analogous MTS structures containing titanium. Results...

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